Articles in this Issue

  • Improving Selection of a CMO for Sterile Products

    Terrence Walsh, Donald C. Singer
    Responsibility in a contractual agreement between two pharmaceutical companies has been indicated as one of the common cGMP (current Good Manufacturing Practices) compliance challenges during this last decade. Yet, the real challenge is much broader and usually more basic than cGMP compliance. This challenge is raised to a high level of risk when selecting and developing collaboration for manufacturing a sterile pharmaceutical product.
  • Industry’s Opportunity for True Site Partnerships

    Christine Pierre
    Partnering among stakeholders has emerged as an essential tactic for improving operational efficiency in the clinical trials sector. Driven by escalating clinical trial timelines, more complex protocols, stalled patient enrollment, and rising costs, this global industry is evolving past traditional outsourcing toward various types of strategic partnerships and collaborations.
  • Proposal of a Disruption Scoring Model for Pharmaceutical Supply Chains

    Verena Brenner, Dr. Michael Hülsmann
    The phenomenon of supply chain disruptions in globalized production and distribution networks has raised many concerns during the last years. In general, such disruptions are understood as unexpected temporal events, which lead to a negative deviation of the process plans [1, 2]. However, disruptions do not only lead to immediate losses of e.g. products, but may also lead to considerable reputation losses [3]. Especially pharmaceutical supply chains, but also food chains experience a high susceptibility to disruptions, due to the special nature of the products.
  • Qualification and Utilization of CRO Partners

    Dennis Jenke, Ph.D.
    As previously published in Part 1 of this series: “Collection, interpretation, and utilization of extractables or leachables (E&L) data are not trivial processes and the scientific and practical requirements for performing these activities may extend beyond the technical and/or resource capacities of many organizations that are required to possess such data. To bridge these knowledge and resource gaps, organizations turn to contract research organizations (CROs) to provide the needed expertise, the needed capacity, or both.” [1]
  • Genotoxic/Mutagenic Impurities Part 3: CMC (Chemistry, Manufacturing and Controls) Overview

    David P. Elder, Ph.D., David J. Snodin, Ph.D.
    This third article in a series on genotoxic/mutagenic impurities (GTIs) will discuss the challenges facing synthetic and analytical chemists as they endeavor to identify and ultimately control levels of these GTIs or PGIs (potentially genotoxic impurities) in drug substance and drug products. GTIs are residual reagents, intermediates, degradation products or by-products of synthesis that have a demonstrated ability to damage DNA, thus having the potential to cause a mutagenic and possibly a carcinogenic response [1]. GTIs are typically electrophilic (e.g. alkyl halides, alkyl sulfonates, epoxides [2]), or can be metabolized to an electrophilic moiety (e.g. aromatic amines, hydrazines [3]) and act predominantly by alkylation of DNA bases. PGIs are compounds containing an alerting structural motif; moieties such as hydrazine, epoxide, aziridine and N-nitrosamine confer a high likelihood of mutagenic activity, whereas others (e.g. N-oxide, carbamate, Michael acceptor, carboxylic acid chloride, methylol) are considered to be either false positives or extremely weak alerts [4].
  • An Interview With James McGibbon, Director Business Development Almac Pharma Services

    The rationale in opening a commercial packaging facility in the US was two-fold. One – demand from our US clients for a flexible, quality-driven commercial packaging partner and two – the Audubon site was readily available. Almac have owned the site in Audubon, PA since 1997. Originally the facility provided contract clinical packaging services that relocated to Almac’s North American Headquarters in Souderton, PA at the beginning of 2011.
  • Recent Quality Issues in Pharmaceutical Compliance: Lessons from Warning Letters

    Scott M. Wheelwright, Ph.D.
    All of us who work in pharmaceuticals in Europe and the US recognize the need for our manufacturing operations to meet compliance requirements. Quality levels that meet or exceed the expectations of our regulators are a given for our operations.
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